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The CO disproportionation reaction appears to be structure sensitive, as the carbon formation rate increases with decreasing Pd particle size. L x '. 2 0 300 400 500 600 Temperature 700 800 / 900 K Flgure 21 Partial dlssoclatlon of CO on a defect-rlch Pd foil, as evldenced by growlng SlMS Pd,C+ and Pd,O* signals upon heating. TPD measurements lndlcate the desorptlon of molecularly adsorbed a-CO, and a p-CO desorptlon state due to recomblnatlon of carbon and oxygen. Data from Reference 147. The main mechanism of CO oxidation over palladium is the Langmuir-Hinshelwoodreaction between adsorbed CO molecules and adsorbed oxygen atoms.

2 0 300 400 500 600 Temperature 700 800 / 900 K Flgure 21 Partial dlssoclatlon of CO on a defect-rlch Pd foil, as evldenced by growlng SlMS Pd,C+ and Pd,O* signals upon heating. TPD measurements lndlcate the desorptlon of molecularly adsorbed a-CO, and a p-CO desorptlon state due to recomblnatlon of carbon and oxygen. Data from Reference 147. The main mechanism of CO oxidation over palladium is the Langmuir-Hinshelwoodreaction between adsorbed CO molecules and adsorbed oxygen atoms. Palladium single crystal studies have shown that this reaction is essentially structure insensitive.

These spectra should be compared with the RhCl, precursor spectra given in Figure 10 (top). The positive SIMS spectra are dominated by a large elemental Rh' peak at mle=103. The contact of Rh with C1 is reflected in the spectrum of the RhCl, precursor by RhC1' clusters, but these do not appear in the spectrum of the catalyst. Instead, other interesting clusters appear: Rho' (mle=119), Rho* (120), RhA1' (130), and Rho; (135). These molecular clusters give an indication of the Rh ligands after adsorption (OH, H20), but may also be due to the contact of the Rh-complexes with the oxidic support.

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Abissi e Inferi by Unknown


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